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STM Investigation of Molecular Architectures of Porphyrinoids on a Ag(111) Surface  Supramolecular Ordering, Electronic Properties and Reactivity  Florian Buchner  Buch  Springer Theses  Englisch - Buchner, Florian
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STM Investigation of Molecular Architectures of Porphyrinoids on a Ag(111) Surface Supramolecular Ordering, Electronic Properties and Reactivity Florian Buchner Buch Springer Theses Englisch - hardcover

2010, ISBN: 9783642148392

[ED: Gebunden], [PU: Springer Berlin], The functionalization of surfaces on the nanoscale is one of the most fascinating and at the same time challenging topics in science. It is the key … More...

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STM Investigation of Molecular Architectures of Porphyrinoids on a Ag(111) Surface - Florian Buchner
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STM Investigation of Molecular Architectures of Porphyrinoids on a Ag(111) Surface - Florian Buchner
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STM Investigation of Molecular Architectures of Porphyrinoids on a Ag(111) Surface - hardcover

2010, ISBN: 3642148395

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STM Investigation of Molecular Architectures of Porphyrinoids on a Ag(111) Surface - Florian Buchner
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STM Investigation of Molecular Architectures of Porphyrinoids on a Ag(111) Surface - hardcover

2010, ISBN: 9783642148392

Supramolecular Ordering, Electronic Properties and Reactivity, Buch, Hardcover, 2010, [PU: Springer Berlin], Springer Berlin, 2010

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STM Investigation of Molecular Architectures of Porphyrinoids on a Ag(111) Surface

The self-assembly of large organic molecules has become a vividly explored and interdisciplinary field in science. One major goal is the tailored fabrication of highly ordered, molecular networks, which are stabilized on a metal surface. Metalloporphyrins receive particular attention, because their distinct intrinsic functionalities make them promising candidates for applications in chemical sensors, solar cells, and for tailored catalytic processes. Based on scanning tunneling microscopy investigations, several novel and fundamental contributions are presented, which has led to a new level of understanding. Highlights are the results with respect to intramolecular conformation and supramolecular ordering, electronic interactions with the substrate, surface confined synthesis such as in-situ metallation reactions, and ligand effects.The number of publications this work has led to emphasises its quality and significance.

Details of the book - STM Investigation of Molecular Architectures of Porphyrinoids on a Ag(111) Surface


EAN (ISBN-13): 9783642148392
ISBN (ISBN-10): 3642148395
Hardcover
Publishing year: 2010
Publisher: Springer Berlin

Book in our database since 2014-02-19T10:42:49-05:00 (New York)
Detail page last modified on 2022-07-24T17:38:38-04:00 (New York)
ISBN/EAN: 9783642148392

ISBN - alternate spelling:
3-642-14839-5, 978-3-642-14839-2


Information from Publisher

Author: Florian Buchner
Title: Springer Theses; STM Investigation of Molecular Architectures of Porphyrinoids on a Ag(111) Surface - Supramolecular Ordering, Electronic Properties and Reactivity
Publisher: Springer; Springer Berlin
164 Pages
Publishing year: 2010-11-11
Berlin; Heidelberg; DE
Printed / Made in
Weight: 0,494 kg
Language: English
139,09 € (DE)
142,99 € (AT)
153,50 CHF (CH)
POD
XXVII, 164 p.

BB; Book; Hardcover, Softcover / Chemie/Physikalische Chemie; Physikalische Chemie; Verstehen; Chemie; Porphyrinoids; STEM; STM; Scanning Tunneling Microscopy; Scanning Tunneling Spectroscopy; Self-assembly; Supra; Supramolecular Chemistry; Surface Chemistry; electronics; B; Physical Chemistry; Analytical Chemistry; Solid State Physics; Surface and Interface Science, Thin Films; Energy Systems; Physical Chemistry; Analytical Chemistry; Condensed Matter Physics; Surface and Interface and Thin Film; Electrical Power Engineering; Mechanical Power Engineering; Chemistry and Materials Science; Analytische Chemie; Physik der kondensierten Materie (Flüssigkeits- und Festkörperphysik); Physik der kondensierten Materie (Flüssigkeits- und Festkörperphysik); Elektrotechnik; Energietechnik, Elektrotechnik und Energiemaschinenbau; BC; EA

1 Introduction ...................................................................................................... 1 2 Fundamentals .................................................................................................... 5 2.1 Principle of the STM ............................................................................................ 5 2.2 Origin of the Tunneling Current ........................................................................... 7 2.3 Scanning Tunneling Spectroscopy ...................................................................... 10 2.4 Contrast Mechanism of Molecular Adsorbates ................................................... 13 2.5 Temperature Programmed Desorption ................................................................ 16 2.6 Low Energy Electron Diffraction ....................................................................... 18 3 Experimental Setup ........................................................................................ 21 3.1 UHV System ...................................................................................................... 21 3.2 Scanning Tunneling Microscope ........................................................................ 23 3.3 Control Electronics and Vibration Isolation ........................................................ 26 3.4 Ag(111) ............................................................................................................. 28 3.5 Porphyrinoids..................................................................................................... 30 3.6 Preparation of thin Porphyrinoid Layers ............................................................. 33 3.7 Vapor-deposition of Cobalt and Iron .................................................................. 34 4 Results ............................................................................................................. 39 4.1 Self-Assembly and Individual Appearance of Tetraphenylporphyrins on Ag(111) ............................................................................................................. 41 4.1.1 Epitaxial growth ........................................................................................... 43 4.1.2 Appearance and Intramolecular Conformation .............................................. 48 4.1.3 Ordering Aspects.......................................................................................... 50 4.2 Self-Assembly and Individual Appearance of Cobalt(II)-Tetrakisditertbutylphenylporphyrins on Ag(111) ......................................................................... 61 4.2.1 Polymorphism of CoTTBPP ......................................................................... 62 4.2.2 Polarity-Dependent Appearance ................................................................... 78 ii Table of Contents 4.3 Coordination of Iron and Cobalt Atoms by Tetraphenylporphyrin Monolayers on Ag(111) and Formation of Metal(II)-Tetraphenylporphyrin ......... 83 4.3.1 Coordination of Post-deposited Iron Atoms by Tetraphenylporphyrin Monolayers ................................................................................................... 85 4.3.2 Coordination of Pre-deposited Iron Atoms by Tetraphenylporphyrin Monolayers ................................................................................................... 90 4.3.3 Coordination of Post-deposited Cobalt Atoms by Tetraphenylporphyrin Monolayers ................................................................................................... 94 4.3.4 Discussion of the Metalation Reaction .......................................................... 99 4.4 Different Aspects of 2H-Tetrakisditertbutylphenylporphyrin on Ag(111) .. 103 4.4.1 Monolayer Preparation................................................................................ 104 4.4.2 Arrangement of 2HTTBPP ......................................................................... 107 4

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